Transcript HOW TO MANAGE EDITORIAL WORK (EDITOR & SECTION …

EXAMPLE
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Example 11.1
A feed to a column has the composition given in the table below,
and is at a pressure of 14 bar and a temperature of 60oC. Calculate
the flow and composition of the liquid and vapour phases. Take the
equilibrium data
Feed
Kmol/h
zi
Ki
ethane (C2)
20
0,25
3.8
propane (C3)
20
0,25
1.3
isobutane (iC4)
20
0,25
0.43
n-pentane (nC5)
20
0,25
0.16
Solution
For two phases to exist the flash temperature must lie between
the bubble point and dew point of the mixture
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Check feed condition
therefore the feed is a two phase mixture
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Flash calculation
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Hengstebeck’s method is used to find the third trial value for L/V.
The calculated values are plotted against the assumed values and
the intercept with a line at 45o (calculated = assumed) gives the
new trial value, 2.4.
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Example 11.2
Acetone is to be recovered from an aqueous waste stream by
continuous distillation. The feed will contain 10 per cent w/w
acetone. Acetone of at least 98 per cent purity is wanted, and the
aqueous effluent must not contain more than 50 ppm acetone. The
feed will be at 20oC. Estimate the number of ideal stages required.
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The equilibrium curve can be drawn with sufficient accuracy to determine the
stages above the feed by plotting the concentrations at increments of 0.1.
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Sensible heat
 for the operating line at minimum reflux = 0.65
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Latent heat
 three stages above the feed up to y = 0.8.
 the stages above y = 0.8: three to four stages required;
 total stages above the feed 7
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 Below the feed, one stage is required down to x = 0.04
 A log-log plot is used to determine the stages below this
concentration.
 Data for log-log plot:
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