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Drying
We are primarily concerned with drying wet, porous solids
(granules).
Important to ensure proper moisture content in the granules:
low enough to prevent product degradation and ensure good
powder flow, but high enough to provide good tablet
properties
B. Amsden
CHEE 440
Definitions
psychrometry
determination of the vapor concentration and carrying
capacity of drying gas
wet bulb T
dry bulb T
relative humidity (RH)
Pwate r in ai r
%RH
100
Pw ,sa t T
moisture content
B. Amsden
CHEE 440
Psychrometric
Chart
Determine the relative
humidity and moisture
content in the air if the
wet bulb T is 35 ºC and
the dry bulb T is 50 ºC.
B. Amsden
CHEE 440
Types of Dryers
B. Amsden
CHEE 440
Static Dryers
Tray/truck driers
B. Amsden
CHEE 440
Drying behavior for static bed
B. Amsden
CHEE 440
Fluidized Bed
B. Amsden
CHEE 440
Spray Dryer
B. Amsden
CHEE 440
Drying Equations
Tray/Truck Dryers
constant rate drying stage only
dm h c AT
=
dt
• parallel flow over a static bed
8.8G 0.8
hc
D 0.2
• perpendicular flow through a bed
Nu 1.17Re 0.585 Pr 0.333
B. Amsden
CHEE 440
Drying Equations
Fluidized beds and spray driers
use correlation for flow past an individual spherical
particle
Nu 2.0 0.61Re 0.5 Pr 0.333
B. Amsden
CHEE 440
Example
Wet granules (density = 1.5 g/cm3) are spread onto a
screen at an amount of 10 kg/m2 of screen. The bed
porosity is 45% and the wet granules have an average
diameter of 300 mm. Air at 60ºC(dry bulb) and a wet
bulb temp of 25ºC is passed through the bed at a
velocity of 0.15 m/s. How long will it take to dry the
granules from 20 to 10 % moisture? The critical
moisture content of the granules is 9 %.
B. Amsden
CHEE 440