Transcript Document

Hi-Speed Refinery Gas Analyzer
AC Analytical Controls
Analysis time:
5 minutes
System characterizes:

All C1 - nC6 hydrocarbons.

Inert gases: including nitrogen, hydrogen, helium,
oxygen, carbon monoxide, carbon dioxide.

Hydrogensulfide, which requires an additional
analysis time of 2 minutes.

The Hi-Speed RGA also characterizes the composition
of LPG and butane streams in only three minutes.
Performance specifications:
The lowest detection limit (LDL) is:

Hydrocarbons: 0.01 mol%

Inert gases: 0.02 mol%

Hydrogensulfide: 0.1 mol%
Column Dimensions:
No. Packing material
1
Methyl silicone
2
Al2O3
3
4
5
6
Dimensions
RUNTABLE
TIME
VALVE ACTION
0.00
0.01
0.01
0.25
0.30
0.45
0.50
0.70
0.70
1.20
2.00
4.99
4.99
SAMPLE FLUSH
V6
Vent He
Vent N2
V2
Vent He
FID
Vent N2
Ref He
Molsieve 13X
Nitrogen
3000
Haysep N
Hydrogen
25 uV
1000
CarbonMonoxide
2000
CarbonDioxide
t-2-Butene
i-Butene 1-Butene
c-2-Butene
i-Pentane
n-Pentane
1,3-Butadiene
t-2-Pentene
2-Methyl-2-Pentene
1 -Pentene
c-2-Pentene
n-Butane
Propadiene
Acetylene
Propylene
V3
Vent
He (Aux 4)
Oxygen
V4
He (Aux 3)
TCD
Ref. N2
Haysep Q
Sample out
C6+
100
Sample in
S/SL
Propame
200
V5
V1
Methane
Ethane
Ethylene
300
N2 (Aux 5)
Haysep Q/MS 5A
ON
ON
ON
ON
OFF
OFF
ON
OFF
ON
OFF
OFF
OFF
pA
0.5 m Meth. Silicone
Front Inlet
i-Butane
1
6
4
5
4
1
2
6
3
3
2
5
15 m Al2O3
0
0
1
2
3
4
min.
1
2
3
4
min.
RUNTABLE
TIME
VALVE ACTION
0.00
0.01
0.01
0.25
0.30
0.45
0.50
0.70
0.70
1.20
2.00
4.99
4.99
SAMPLE FLUSH
V6
Vent He
Vent N2
V2
Vent He
FID
Vent N2
Ref He
Molsieve 13X
Nitrogen
3000
Haysep N
Hydrogen
25 uV
1000
CarbonMonoxide
2000
CarbonDioxide
t-2-Butene
i-Butene 1-Butene
c-2-Butene
i-Pentane
n-Pentane
1,3-Butadiene
t-2-Pentene
2-Methyl-2-Pentene
1 -Pentene
c-2-Pentene
n-Butane
Propadiene
Acetylene
Propylene
V3
Vent
He (Aux 4)
Oxygen
V4
He (Aux 3)
TCD
Ref. N2
Haysep Q
Sample out
C6+
100
Sample in
S/SL
Propame
200
V5
V1
Methane
Ethane
Ethylene
300
N2 (Aux 5)
Haysep Q/MS 5A
ON
ON
ON
ON
OFF
OFF
ON
OFF
ON
OFF
OFF
OFF
pA
0.5 m Meth. Silicone
Front Inlet
i-Butane
1
6
4
5
4
1
2
6
3
3
2
5
15 m Al2O3
0
0
1
2
3
4
min.
1
2
3
4
min.
RUNTABLE
TIME
VALVE ACTION
0.00
0.01
0.01
0.25
0.30
0.45
0.50
0.70
0.70
1.20
2.00
4.99
4.99
SAMPLE FLUSH
V6
Vent He
Vent N2
V2
Vent He
FID
Vent N2
Ref He
Molsieve 13X
Nitrogen
3000
Haysep N
Hydrogen
25 uV
1000
CarbonMonoxide
2000
CarbonDioxide
t-2-Butene
i-Butene 1-Butene
c-2-Butene
i-Pentane
n-Pentane
1,3-Butadiene
t-2-Pentene
2-Methyl-2-Pentene
1 -Pentene
c-2-Pentene
n-Butane
Propadiene
Acetylene
Propylene
V3
Vent
He (Aux 4)
Oxygen
V4
He (Aux 3)
TCD
Ref. N2
Haysep Q
Sample out
C6+
100
Sample in
S/SL
Propame
200
V5
V1
Methane
Ethane
Ethylene
300
N2 (Aux 5)
Haysep Q/MS 5A
ON
ON
ON
ON
OFF
OFF
ON
OFF
ON
OFF
OFF
OFF
pA
0.5 m Meth. Silicone
Front Inlet
i-Butane
1
6
4
5
4
1
2
6
3
3
2
5
15 m Al2O3
0
0
1
2
3
4
min.
1
2
3
4
min.
RUNTABLE
TIME
VALVE ACTION
0.00
0.01
0.01
0.25
0.30
0.45
0.50
0.70
0.70
1.20
2.00
4.99
4.99
SAMPLE FLUSH
V6
Vent He
Vent N2
V2
Vent He
FID
Vent N2
Ref He
Molsieve 13X
Nitrogen
3000
Haysep N
Hydrogen
25 uV
1000
CarbonMonoxide
2000
CarbonDioxide
t-2-Butene
i-Butene 1-Butene
c-2-Butene
i-Pentane
n-Pentane
1,3-Butadiene
t-2-Pentene
2-Methyl-2-Pentene
1 -Pentene
c-2-Pentene
n-Butane
Propadiene
Acetylene
Propylene
V3
Vent
He (Aux 4)
Oxygen
V4
He (Aux 3)
TCD
Ref. N2
Haysep Q
Sample out
C6+
100
Sample in
S/SL
Propame
200
V5
V1
Methane
Ethane
Ethylene
300
N2 (Aux 5)
Haysep Q/MS 5A
ON
ON
ON
ON
OFF
OFF
ON
OFF
ON
OFF
OFF
OFF
pA
0.5 m Meth. Silicone
Front Inlet
i-Butane
1
6
4
5
4
1
2
6
3
3
2
5
15 m Al2O3
0
0
1
2
3
4
min.
1
2
3
4
min.
RUNTABLE
TIME
VALVE ACTION
0.00
0.01
0.01
0.25
0.30
0.45
0.50
0.70
0.70
1.20
2.00
4.99
4.99
SAMPLE FLUSH
V6
Vent He
Vent N2
V2
Vent He
FID
Vent N2
Ref He
Molsieve 13X
Nitrogen
3000
Haysep N
Hydrogen
25 uV
1000
CarbonMonoxide
2000
CarbonDioxide
t-2-Butene
i-Butene 1-Butene
c-2-Butene
i-Pentane
n-Pentane
1,3-Butadiene
t-2-Pentene
2-Methyl-2-Pentene
1 -Pentene
c-2-Pentene
n-Butane
Propadiene
Acetylene
Propylene
V3
Vent
He (Aux 4)
Oxygen
V4
He (Aux 3)
TCD
Ref. N2
Haysep Q
Sample out
C6+
100
Sample in
S/SL
Propame
200
V5
V1
Methane
Ethane
Ethylene
300
N2 (Aux 5)
Haysep Q/MS 5A
ON
ON
ON
ON
OFF
OFF
ON
OFF
ON
OFF
OFF
OFF
pA
0.5 m Meth. Silicone
Front Inlet
i-Butane
1
6
4
5
4
1
2
6
3
3
2
5
15 m Al2O3
0
0
1
2
3
4
min.
1
2
3
4
min.
RUNTABLE
TIME
VALVE ACTION
0.00
0.01
0.01
0.25
0.30
0.45
0.50
0.70
0.70
1.20
2.00
4.99
4.99
SAMPLE FLUSH
V6
Vent He
Vent N2
V2
Vent He
FID
Vent N2
Ref He
Molsieve 13X
Nitrogen
3000
Haysep N
Hydrogen
25 uV
1000
CarbonMonoxide
2000
CarbonDioxide
t-2-Butene
i-Butene 1-Butene
c-2-Butene
i-Pentane
n-Pentane
1,3-Butadiene
t-2-Pentene
2-Methyl-2-Pentene
1 -Pentene
c-2-Pentene
n-Butane
Propadiene
Acetylene
Propylene
V3
Vent
He (Aux 4)
Oxygen
V4
He (Aux 3)
TCD
Ref. N2
Haysep Q
Sample out
C6+
100
Sample in
S/SL
Propame
200
V5
V1
Methane
Ethane
Ethylene
300
N2 (Aux 5)
Haysep Q/MS 5A
ON
ON
ON
ON
OFF
OFF
ON
OFF
ON
OFF
OFF
OFF
pA
0.5 m Meth. Silicone
Front Inlet
i-Butane
1
6
4
5
4
1
2
6
3
3
2
5
15 m Al2O3
0
0
1
2
3
4
min.
1
2
3
4
min.
RUNTABLE
TIME
VALVE ACTION
0.00
0.01
0.01
0.25
0.30
0.45
0.50
0.70
0.70
1.20
2.00
4.99
4.99
SAMPLE FLUSH
V6
Vent He
Vent N2
V2
Vent He
FID
Vent N2
Ref He
Molsieve 13X
Nitrogen
3000
Haysep N
Hydrogen
25 uV
1000
CarbonMonoxide
2000
CarbonDioxide
t-2-Butene
i-Butene 1-Butene
c-2-Butene
i-Pentane
n-Pentane
1,3-Butadiene
t-2-Pentene
2-Methyl-2-Pentene
1 -Pentene
c-2-Pentene
n-Butane
Propadiene
Acetylene
Propylene
V3
Vent
He (Aux 4)
Oxygen
V4
He (Aux 3)
TCD
Ref. N2
Haysep Q
Sample out
C6+
100
Sample in
S/SL
Propame
200
V5
V1
Methane
Ethane
Ethylene
300
N2 (Aux 5)
Haysep Q/MS 5A
ON
ON
ON
ON
OFF
OFF
ON
OFF
ON
OFF
OFF
OFF
pA
0.5 m Meth. Silicone
Front Inlet
i-Butane
1
6
4
5
4
1
2
6
3
3
2
5
15 m Al2O3
0
0
1
2
3
4
min.
1
2
3
4
min.
RUNTABLE
TIME
VALVE ACTION
0.00
0.01
0.01
0.25
0.30
0.45
0.50
0.70
0.70
1.20
2.00
4.99
4.99
SAMPLE FLUSH
V6
Vent He
Vent N2
V2
Vent He
FID
Vent N2
Ref He
Molsieve 13X
Nitrogen
3000
Haysep N
Hydrogen
25 uV
1000
CarbonMonoxide
2000
CarbonDioxide
t-2-Butane
i-Butene 1-Butene
c-2-Butene
i-Pentane
n-Pentane
1,3-Butadiene
t-2-Pentene
2-Methyl-2-Pentene
1-Pentene
c-2-Pentene
n-Butane
Propadiene
Acetylene
Propylene
V3
Vent
He (Aux 4)
Oxygen
V4
He (Aux 3)
TCD
Ref. N2
Haysep Q
Sample out
C6+
100
Sample in
S/SL
Propane
200
V5
V1
Methane
Ethane
Ethylene
300
N2 (Aux 5)
Haysep Q/MS 5A
ON
ON
ON
ON
OFF
OFF
ON
OFF
ON
OFF
OFF
OFF
pA
0.5 m Meth. Silicone
Front Inlet
i-Butane
1
6
4
5
4
1
2
6
3
3
2
5
15 m Al2O3
0
0
1
2
3
4
min.
1
2
3
4
min.
RUNTABLE
TIME
VALVE ACTION
0.00
0.01
0.01
0.25
0.30
0.45
0.50
0.70
0.70
1.20
2.00
4.99
4.99
SAMPLE FLUSH
V6
Vent He
Vent N2
V2
Vent He
FID
Vent N2
Ref He
Molsieve 13X
Nitrogen
3000
Haysep N
Hydrogen
25 uV
1000
CarbonMonoxide
2000
CarbonDioxide
t-2-Butene
i-Butene 1-Butene
c-2-Butene
i-Pentane
n-Pentane
1,3-Butadiene
t-2-Pentene
2-Methyl-2-Pentene
1 -Pentene
c-2-Pentene
n-Butane
Propadiene
Acetylene
Propylene
V3
Vent
He (Aux 4)
Oxygen
V4
He (Aux 3)
TCD
Ref. N2
Haysep Q
Sample out
C6+
100
Sample in
S/SL
Propame
200
V5
V1
Methane
Ethane
Ethylene
300
N2 (Aux 5)
Haysep Q/MS 5A
ON
ON
ON
ON
OFF
OFF
ON
OFF
ON
OFF
OFF
OFF
pA
0.5 m Meth. Silicone
Front Inlet
i-Butane
1
6
4
5
4
1
2
6
3
3
2
5
15 m Al2O3
0
0
1
2
3
4
min.
1
2
3
4
min.
RUNTABLE
TIME
VALVE ACTION
0.00
0.01
0.01
0.25
0.30
0.45
0.50
0.70
0.70
1.20
2.00
4.99
4.99
SAMPLE FLUSH
V6
Vent He
Vent N2
V2
Vent He
FID
Vent N2
Ref He
Molsieve 13X
Nitrogen
3000
Haysep N
Hydrogen
25 uV
1000
CarbonMonoxide
2000
CarbonDioxide
t-2-Butene
i-Butene 1-Butene
c-2-Butene
i-Pentane
n-Pentane
1,3-Butadiene
t-2-Pentene
2-Methyl-2-Pentene
1 -Pentene
c-2-Pentene
n-Butane
Propadiene
Acetylene
Propylene
V3
Vent
He (Aux 4)
Oxygen
V4
He (Aux 3)
TCD
Ref. N2
Haysep Q
Sample out
C6+
100
Sample in
S/SL
Propame
200
V5
V1
Methane
Ethane
Ethylene
300
N2 (Aux 5)
Haysep Q/MS 5A
ON
ON
ON
ON
OFF
OFF
ON
OFF
ON
OFF
OFF
OFF
pA
0.5 m Meth. Silicone
Front Inlet
i-Butane
1
6
4
5
4
1
2
6
3
3
2
5
15 m Al2O3
0
0
1
2
3
4
min.
1
2
3
4
min.