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Kevin Cowtan, [email protected]

CCP4 Wiki ccp4wiki.org

Maintainer: YOU

CCP4 DevMeet

CCP4 wiki

Original aims (as I understand them):  Provide a framework for updating the documentation.

 Provide a forum for useful BB discussions to be collected.

Kevin Cowtan, [email protected]

CCP4 DevMeet

CCP4 wiki

Provide a forum for useful BB discussions to be collected.

 Addressed by Kay Diedrichs with the CCP4 community wiki!

 Less work for us!

 Publicly editable. (vs our more restricted aims)  Independent. (No legal ramifications for us) Kevin Cowtan, [email protected]

CCP4 DevMeet

CCP4 wiki

Provide a framework for updating the documentation.

 A wiki has been setup and configured using an external web hosting service.

 Took 2 attempts, but the new host seems good. Don't know about support, I haven't needed it!

 Populated with a few demonstration pages to provide ideas and inspiration.

Kevin Cowtan, [email protected]

CCP4 DevMeet

Kevin Cowtan, [email protected]

CCP4 DevMeet

Kevin Cowtan, [email protected]

CCP4 DevMeet

Kevin Cowtan, [email protected]

CCP4 DevMeet

Kevin Cowtan, [email protected]

CCP4 DevMeet

Kevin Cowtan, [email protected]

CCP4 DevMeet

Kevin Cowtan, [email protected]

CCP4 DevMeet

Kevin Cowtan, [email protected]

CCP4 DevMeet

Kevin Cowtan, [email protected]

CCP4 DevMeet

Kevin Cowtan, [email protected]

CCP4 DevMeet

CCP4 Wiki

And Kevin said ... 'Go forth and edit'

Kevin Cowtan, [email protected]

CCP4 DevMeet

WP5

Model Building, Refinement and Ligands Kevin Cowtan, Garib Murshudov, Paul Emsley Raj Pannu Nick Furnham

Kevin Cowtan, [email protected]

CCP4 DevMeet

WP goals from Sep 07

4 sets of goals:  Buccaneer goals  Refmac goals  Coot goals  Collaborative goals Kevin Cowtan, [email protected]

CCP4 DevMeet

WP goals from Sep 07

Buccaneer goals:  Improve chain numbering (done, 6.1)  Improve sidechain building (done, 6.1)  Fix model position (done, 6.1) 

Implement sequence verification

Kevin Cowtan, [email protected]

CCP4 DevMeet

WP goals from Sep 07

Refmac goals: 

Better communication with Coot. (done)

Release refinement against SAD target. (6.1 uns)

First release of JLigand. (6.1?, to be released)

Twin refinement. (to be released)

Flexible NCS, occupancy, B restraints.

GUI pipeline options for waters, blast, etc.

Sensible GUI defaults for TLS.

Kevin Cowtan, [email protected]

CCP4 DevMeet

WP goals from Sep 07

Coot goals:  Integrate wincoot. (done) 

Test new Ramachandran restraint idea. (nearly)

Use MMDB link-reading code. (license)

Rapper wrapper. (nearly)

Kevin Cowtan, [email protected]

CCP4 DevMeet

WP goals from Sep 07

Collaborative goals: 

Decide what to do about ligand developments.

PE/GM.

Buccaneer/refmac recycling to make better use of refmac.

KC/GM teaching, other work.

Make contact with new Rapper developer.

 (visa issues) Kevin Cowtan, [email protected]

CCP4 DevMeet

Buccaneer

The buccaneer software for automated model building of protein structures across a broad range of resolutions.

Kevin Cowtan YSBL, University of York

[email protected]

Kevin Cowtan, [email protected]

CCP4 DevMeet

Buccaneer

Buccaneer 1.0 (for CCP4 v6.1)    A few, very major developments: Buccaneer-Refmac pipeline NCS auto-completion Improved sequencing Kevin Cowtan, [email protected]

CCP4 DevMeet

Buccaneer: Future

Buccaneer 1.1 (ready for release after 6.1)  Improved linking of nearby chains  Improved numbering of output chains  Improved sidechain fitting:     Use Richardson rotamer library Favour more probable sidechain rotamers Rudimentary chi1 refinement Prune clashing side chains  Optionally fix the model in the ASU  General performance improvements (33%) 

Multi-threading (for dual/quad core machines)

Kevin Cowtan, [email protected]

CCP4 DevMeet

Buccaneer: Future

Buccaneer 1.2+  Rebuilding cis-peptides, pep-flips, pep-rots.

 Sequence verification.

 Use of Se atoms, MR model in sequencing.

 Loop building.

B-factor refinement. (Also for coot)

Kevin Cowtan, [email protected]

CCP4 DevMeet

Buccaneer: Comparisons

With ARP/wARP:  From my tests and user reports buccaneer will build most structures which ARP/wARP will build.

 But ARP/wARP gets a lower R-factor.

 The benefit of using individual atoms.

 Buccaneer will also build structures where ARP/wARP fails.

 Particularly with good data but poor resolution.

 The benefit of using larger rigid groups.

Kevin Cowtan, [email protected]

CCP4 DevMeet

Buccaneer: Comparisons

Citations:  Still only 4.

(structures published without citation - grrr...) User reports:  2 novel structures built at 3.6A

 1 commercial MR structure rebuilt at York at 3.1A

(Buccaneer/Coot/Quanta) Kevin Cowtan, [email protected]

CCP4 DevMeet

Buccaneer: Comparisons

User reports: 

Pietro Roversi:

 Used for 2vix.

 Recommends it for the range 2.6-3.2A.

Tassos Perrakis:

 Currently using it for tricky MR rebuild at 2.7A

Qui Ping Xu (JCSG):

 Builds 2.8A structures where RESOLVE fails.

 Incorporate in JCSG pipeline.

Clemens Vonrhein: ...

Kevin Cowtan, [email protected]

CCP4 DevMeet

Buccaneer and density modification

Clemens:  Iteration of buccaneer and solomon shows promise.

 Traditional density modification still has much to offer.

By contrast with Pirate:  Other developers have not on the whole had much success with Pirate.

 The statistical dm calculation is far harder to analyse. A development black hole.

Kevin Cowtan, [email protected]

CCP4 DevMeet

Buccaneer and density modification

Parrot:  Traditional density modification (c.f. Solomon), with some new elements:  MLHL target (under development for use in coot).

 Refine alpha, beta, and the parameters of the solvent mask against the free LLK.

 Later, more advanced elements can be introduced. Prior density information from:  Atomic model from MR/Buccaneer  NCS (automated), from either HA or partial model.

Kevin Cowtan, [email protected]

CCP4 DevMeet

Buccaneer and density modification

Parrot:  A stand-alone density modification program:  Like 'dm', but more automated.

 Fast.

 A step within buccaneer:  No prior density modification step required.

 Recycling allows model to be used as prior density and to identify NCS.

Kevin Cowtan, [email protected]

CCP4 DevMeet

Achnowledgements

Help:

JCSG data archive: www.jcsg.org

Paul Emsley, Eleanor Dodson

Randy Read, Clemens Vonrhein Funding:

The Royal Society

Kevin Cowtan, [email protected]

CCP4 DevMeet