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MATERIAL RESPONSE TO MICROSTRUCTURAL-, MECHANICAL- AND THERMAL- STIMULI Stream: Mechanical Engineering Dr. Kantesh Balani (Materials Science & Engineering, IIT Kanpur) Objective : “To elicit material’s response to microstructural-, mechanical-, and thermal- stimuli.” Experiments Originally Proposed: - Been revised for appealing to UG students - More component of fundamentals included - Pictorial graphs and bullets of conclusions are added for clarity Status: Demo of 6 expt. over the internet in virtual mode. Under Progress: 1. Fluorescence Microscopy/ Wetting Phenomena 2. Views / reports on any user trials / field tests carried out. Meetings: To meet DNC on Mar. 18/19 IIT Kharagpur at Kolkata Website http://home.iitk.ac.in/~kbalani/vl-kb/Home%20page.html Apr. 18, 2011 Objectives To elicit material’s response to stimuli of: Creep Nanoindentation Flourescence Microscopy Wetting Ionic Conductivity Thermal + Load Mechanical Response Biological Surface Response Surface Response Conductivity Dr. Kantesh Balani Virtual Lab on Material Response Apr. 18 2011 Introduction/Aim Most materials are seen to behave very similarly w.r.t time dependent deformation. These general features are common to many materials with varied crystal structures, strengthening mechanisms, and strength levels. Our aim is to develop virtual lab experiemtns for how materials respond in general with respect to stimulus of: Creep (Thermal + Load) Mechanical (Loading) Biological (To Cells) Wetting (Surface Response) Conductivity (Ionic at Various Temperatures) Dr. Kantesh Balani Virtual Lab on Material Response Apr. 18 2011 Creep and Its Features Stage I Dislocation Climb away from obstacles Stage II Rate of Dislocation climb equals that of blocking by obstacles Stage III Necking occurs, stress increases http://home.iitk.ac.in/~kbalani/vl-kb/creep1.html Dr. Kantesh Balani Virtual Lab on Material Response Apr. 18 2011 Utilizing Mechanism of Load Transfer There will be a spectrum of obstacle‘ strengths’ that resist local deformation. The model is based on the idea of simply(if approximately) linking many independent and simply described elements into a macroscopic ‘whole’. The model developed here stems from the theory of thermally activated plastic deformation. It naturally produces the types of transients observed on the immediate loading of materials (primary creep) In the model’s present form, strain hardening and recovery processes are not considered. Dr. Kantesh Balani Virtual Lab on Material Response Apr. 18 2011 Nanoindentation Nanoindentation to investigate mechanical properties: (i) Hardness (ii) Elastic modulus (iii) Plasticity index Hardness is proportional to the applied load P divided by the area of contact surface Elastic deformation occurs due to the stretching of the bonds and comes back to the original shape upon removal of loading http://home.iitk.ac.in/~kbalani/vl-kb/nano.html Experiments Completed CREEP: Experiment 1 : Creep Transient Based on Material Selection (Pt/Mg) Experiment 2 : Selection of Obstacle Distance (λ, grain boundary or precicipitate) Experiment 3 : Selection of Obstacle Density (ρ,number of grains/precipitates) NANOINDENTATION: Experiment 4 : Hardness & Modulus Experiment 5: Indent Depth Experiment 6: Plastic Work http://home.iitk.ac.in/~kbalani/vl-kb/Home%20page.html Dr. Kantesh Balani Virtual Lab on Material Response Apr. 18 2011 User Reports Will showcase this website on Apr. 19th to students of CSJM University (Kanpur). Feedbacks: Creep Experiment is fine Polymer Characterization can be added (mainly FTIR) Nanoindentation of polymeric composite Will show surface energy by contact angle measurement Biological property of polymeric materials will be elicited (Fluorescence microscopy) To Be Accomplished Stage II: Completing rest set of experiments Fluorescence microscopy for biological response of material (Two Experiments) Wetting of material by varying its composition (Two Experiments) Ionic Conductivity at different temperatures (Two Experiments) Dr. Kantesh Balani Virtual Lab on Material Response Apr. 18 2011 Thank You