Transcript Folie 1

LAB COURSE
in
GENERAL CHEMISTRY
WS 2011
8.11.2010
PRELIMINARY MEETING
Some organisational stuff
Requirement:
INTRODUCTION TO GENERAL CHEMISTRY 1
EINFÜHRUNG IN DIE ALLGEMEINE CHEMIE 1
Some organisational stuff
CatchUp-Exam on Thursday
Some organisational stuff
Is anyone here who actually doesn‘t
want to attend the lab course?
Number of Workbenches
Number of Workbenches
How many students absolved the exam of
„Introduction in General Chemistry 1“
in former years and want to attend
this years lab course?
• Lab?
• Just Exam(s)?
Number of Workbenches
HTL or similar practical education
 You have to write the intermediate exams
every Tuesday at 12.45 pm!
 You don‘t have to do the practical work in
the lab!
 You have to write the final exam!
Number of Workbenches
HTL or similar practical education?
• Fill in on list
• Copy of final certificate
(until next week)
SUPERVISORS
Dipl.Ing. Sebastian Leitner
Dipl.Ing. Michael König
Dipl.Ing. Kerstin Oppelt
Dipl.Ing. Lorenz Reith
Dipl.Ing. Christa Hirtenlehner
Dipl.Ing. Eva Wöß
CONTACT DATA
Office:
TNF-Tower
T533
Phone:
+43 732 2468 9368
intern just 9368
Mail:
[email protected]
Homepage: www.anorganik.jku.at
ATTENDANCE
Our course is a so called
PRACTICAL COURSE
University law says: a practical course is a
course with compulsory attendance and
immanent exam situation
ATTENDANCE
Physical presence is obligatory!
• Noone who misses this lecture or the fire
lecture can attend the lab course!
• If you are ill, we need to see a doctors
note!
• Tell us BEFORE a lab day starts if you are
ill -> CONTACT DATA!
SCHEDULE
• Preliminary meeting
• Fire lecture and
Place takeover
today
next week
• 5 weeks of lab work with intermediate exams
• 1 week for work-up, cleaning and
place returning
• Final exam
SCHEDULE
Preliminary Meeting
Exam in Introduction
to General Chemistry 1
Fire Lecture
Place takeover
1 Lab-week
Tuesday-Thursday
1st day Intermediate Exam
12.45
Lab-weeks
Place cleaning and returning
Final exam
3 days of labwork
Monday of the following
Week until 12 am:
PROTOCOLS
T533
SCHEDULE
Labday
12.45-17:45 Uhr
12:45 – 13.00
Meeting with your supervisor in the
Lab and discussion in groups of about
10 students + supervisor of todays labwork
NO ONE STARTS ANY EXPERIMENTS BEFORE!
TIME IS PRECIOUS – BE ON TIME
13:00 – 17:00 Uhr
Labwork
WE FEEL FREE TO CHECK YOUR KNOWLEDGE
ABOUT CURRENT EXPERIMENTS!
17:00 – 17:45 Uhr
Cleaning and Final check
SIGN-OUT!
SCHEDULE
SCHEDULE
Students with
prior practical
education
other students
22.11.2011
22.11.2011
29.11.2011
29.11.2011
06.12.2011
06.12.2011
13.12.2011
13.12.2011
10.01.2012
10.01.2012
Intermediate
exams
labwork
NONE
Nov/Dec/Jan
Final exam
(catch up)
20th January 2011 HS7
20th January 2011 HS7
12.00
12.00
31th January 2011 HS12
31th January 2011 HS12
12.45
12.45
SCRIPTS & EXAMINATION MATTER
www.anorganik.jku.at
SCRIPTS & EXAMINATION MATTER
www.anorganik.jku.at
SCRIPTS & EXAMINATION MATTER
•
Guide for Laboratory in General Chemistry
Praktikum aus Allgemeiner Chemie
SCRIPTS & EXAMINATION MATTER
•
Guide for Laboratory in General Chemistry
Praktikum aus Allgemeiner Chemie
SCRIPTS & EXAMINATION MATTER
•
Guide for Laboratory in General Chemistry
Praktikum aus Allgemeiner Chemie
SCRIPTS & EXAMINATION MATTER
•
Guide for Laboratory in General Chemistry
Praktikum aus Allgemeiner Chemie
•
Primer (English)
Primer (Deutsch)
SCRIPTS & EXAMINATION MATTER
•
Guide for Laboratory in General Chemistry
Praktikum aus Allgemeiner Chemie
•
Primer (English)
Primer (Deutsch)
•
Supporting Information:
MSDS
Laboratory Regulations
Fire Issues
PASSWORD
MARKING
•
•
•
•
Practical work
Protocols
Intermediate exams
Final exam
EXCLUSION CRITERIA
• Experimental work: Insufficient practical work leads to
exclusion from the laboratory course. Therefore a judging
scheme exists: If you have to repeat a protocol you get one
negative entry, if you have to repeat an experiment you get
two negative entries. If the number of negative entries
exceeds eight, you are excluded from the laboratory course.
• Behaviour: A major offense against the laboratory
regulations leads to exclusion from the laboratory course. A
minor offense against the regulations leads to a negative
entry in the “don’t exceed the eight entries”-scheme
mentioned above!
• Weekly exams: If you fail twice in the weekly exams you
are excluded from the laboratory course.
LABORATORY REGULATIONS
Download:
On our HP in English and German!
Read it, obey it!
Next week you have to sign a list:
“With your signature you confirm your participation
at the lab course “Laboratory in General
Chemistry” and you accept the laboratory rules!”
LABORATORY PROTOCOLS
You need a (big) book for laboratory
protocols which you have to write by hand,
and a laboratory journal (small book) for
notes in the lab.
No practical guide is allowed in the lab!
How to write a protocol will be discussed
during labcourse!
LaborORDNUNG / TIDYNESS
WRONG!
CORRECT!
Bottles and flasks marked with content
name and place number (permanent
marker)
Removed dirty glassware that is not
longer use
Closed chemical containers
SAFETY CLOTHING
Lab coat

Lab goggles

Suitable gloves

Long hair tied together

LAB EQUIPMENT
Lab coat
Safety goggles
Spatulas (big and small)
Peleus ball
Gloves (butyl nitrile,
neoprene)
Cleaning equipment
(sponge, cleaning
agent, kitchen paper)
Permanent marker
Calculator
Lab journal
Protocol book
LAB EQUIPMENT
Lab coat
Safety goggles
Spatulas (big and small)
Peleus ball
Gloves (butyl nitrile,
neoprene)
Cleaning equipment
(sponge, cleaning
agent, kitchen paper)
Sold at Laboratory Place Takeover!
Lab journal
Protocol book
Permanent marker
Calculator
LAB EQUIPMENT
Lab coat
Safety goggles
Spatulas (big and small)
Peleus ball
Gloves (butyl nitrile,
neoprene)
You need your full
equipment
each Lab-work-Day
starting with
22.11.2011!
Cleaning equipment
(sponge, cleaning
agent, kitchen paper)
Permanent marker
Calculator
Lab journal
Protocol book
EMERGENCY NUMBERS
● Portier (internal phone call) 9100
● fire brigade: 8122 (internal phone)
● police: 8133 (internal phone)
● ambulance: 8144 (internal phone)
● 112 (EU emergency call)
● cell phone: 0732/2468 8122 (e.g.)