Transcript the best dedicated THGA furnace system AAnalyst 600 AA
AAnalyst 600
ES Hwang Inorganic Product Specialist PerkinElmer Korea
AAnalyst 600…
Features
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Dedicated THGA furnace High sensitivity segmented solid-state photodiode detector Simultaneous measurement of sample and reference beams
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Transversely heated graphite furnace
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Longitudinal Zeeman effect background correction
Benefits
THGA furnace reduces interferences in difficult matrices
Exceptional analytical performance and detection limits
Highest Long-term Stability
Minimized interferences and memory effects
Shorter analysis time (fast furnace programs)
Best possible background correction with no light loss
… the best dedicated THGA furnace system
AAnalyst 600
AA Spectrometers
AAnalyst 600
Revolutionary Optical System
AAnalyst 600
Unique Features
First AA spectrometer •
Integrated furnace
Zeeman-THGA graphite furnace
AAnalyst 600
Unique Features
First AA spectrometer •
8-lamp holder
Automatic lamp selection and adjustment
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Built-in power supplies
Hollow cathode lamps
Electrodeless discharge lamps
AAnalyst 600
Highly Versatile Furnace Autosampler
User Benefits:
Automatic generation of reference solutions
Automatic multiple injections
Automatic dilution
Automatic injection into a preheated tube
Variable pipetting speed
Ease-of-operation
AAnalyst 600
Revolutionary Optical System
Real time double beam system
High sensitivity segmented solid-state photodiode detector
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User Benefits:
Exceptional analytical performance
Highest Long-term Stability
AAnalyst 600
Customized Solid-State Detector
Highest quantum efficiency Integrated low noise CMOS charge amplifier array Exceptional signal-to-noise ratio
AAnalyst 600
Quantum Efficiency of Detectors
solid state detector photomultiplier
AAnalyst 600
Furnace (THGA) Instrument Detection Limits
THGA Instrument detection limits (IDL) / pg Element PMT Photodiode As Cr 9 1.5
6 0.4
Cu Mn Pb Tl 5 2 3 7.5
4 1.5
3 7
AAnalyst 600
Automatic Lamp Selector
8-Lamp holder Built-in power supplies for hollow cathode and electrodeless discharge lamps Automatic alignment, element, wavelength and slit selection
AAnalyst 600
Unique Overall Conception
Total system control via AA WinLab32 software for highest versatility and simplest operating convenience
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Atomizer control Lamp and lamp current control THGA control Accessory control
AAnalyst 600
Unique Software Conception
Automatic system setup from stored user’s methods
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Direct from Workspace
Method
Sample information
Individual screen design, window selection etc.
User Benefits:
Analytical reliability
Ease-of-operation
Time-saving
WinLab32 for AA
Bringing a new level of productivity to high-performance AA
AA WinLab32 - Features and Benefits
Improve productivity
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Data Reprocessing * WinLab32 Offline * Priority samples * Append to Analysis List * Edit Calibration Recall Calibration Furnace Method Development wizard *
Improve ease of use and reduce training
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Tool tips (available in 6 languages) * Wizards * Analysis List * AS-93 parameters integrated * * New features not present in 16-bit AA WinLab
AA WinLab32 - Features and Benefits
Reduce training and support
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Common look and feel with WinLab32 for ICP-OES CD Document Pack
Improve stability and data accessibility
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Access database *
Method and data security
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Password protection * Multiple user levels * Data check sums to detect changes * 21 CFR Part 11 Compliant * New features not present in 16-bit AA WinLab
WinLab32 for AA Workspace
Toolbar Automated Analysis Status Monitor Results Calibration
Common look and feel with WinLab32 for ICP for easy cross platform training
Data Reprocessing
Recalculation of analytical data
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Correct SIF errors Change calibration function Delete replicate(s) Performed using the raw data Samples can be reprocessed in any sequence Original data are preserved Analytical log can be printed Reprocessed data are identified
Data Reprocessing
Status display Select samples in the order you want them reprocessed.
Change sample information in these columns
Furnace Method Development Wizard
Define Furnace Steps to cycle Temperatures Analyze Solutions and Display Results
Align Autosampler Tip Wizard
Auto dilution by system
Priority Sample
Samples can be added without interrupting current analyses
Exporting Data to LABWORKS
WinLab32 Enhanced Security Option
Enhancement to WinLab32 for AA (and ICP) Significant set of new features
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Audit trails File versioning Enable compliance with new regulations
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21 CFR Part 11 - Pharmaceutical 40 CFR Part 3 - Environmental (proposed) Others Primarily for highly regulated laboratories
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Users actions are restricted
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Increased storage space requirements Additional information entry requirements Requires more system housekeeping
AAnalyst 600
Total Range Graphite Furnace AA
THGA-type furnace with Zeeman-effect background correction
User Benefits:
Selection of the best system for individual requirements and budgets
High performance, near interference-free trace analysis with STPF concept
AAnalyst 600
Integrated THGA Furnace System
AAnalyst 600
Zeeman THGA Furnace
Transversely heated graphite furnace
Longitudinal Zeeman effect background correction User Benefits:
Exceptional detection limits
Minimized interferences and memory effects
Best possible background correction
Mimimum sample preparation time
Shorter analysis time (fast furnace programs)
AAnalyst 600
Integrated THGA System
THGA Concept: more than 2500 systems in use Longitudinal Zeeman Effect: highly resolved background compensation without light loss DC furnace power supply Closest approach to the "ideal system"
AAnalyst 600
Integrated THGA System
0 .1 2 5 0 .1 0 0 0 .0 7 5 0 .0 5 0 0 .0 2 5 0 .0 0 0 0 1 2
Atomic and background signals for Ba, 20uL, 25 ug/L
A A -B G B G 3 4 T im e / s 5 6 7 8
AAnalyst 600
Zeeman versus D
2 Background Correction
Background correction independent of wavelength True double-beam with only one optical path Baseline noise at least 2x lower Optical resolution
Dl
is 100x better Char. mass typically 10 and 20 % poorer than with D 2 m 0 for the worst case, Cu, is 50% poorer) (the Zeeman-effect background correction gives superior detection limits in real samples
AAnalyst 600
Highly Versatile Furnace Autosampler
High-capacity, interchangeable sample trays
88 or 146 sample positions
Full AA WinLab32 control including multi-tasking
User Benefits:
Automatic generation of reference solutions
Automatic multiple injections
Automatic dilution
Automatic injection into a preheated tube
Variable pipetting speed
Ease-of-operation
AAnalyst 600
Flow Injection - Furnace Coupling
Optional accessory for coupling FI-MHS with furnace AA
Software controlled automatic operation User Benefits:
Detection limits in range of ng/L
Time-savings by automatic on-line operation
Less interferences since matrix components are removed in the FI system
AAnalyst 600
Automatic Slurry Sampling
Optional ultrasonic probe integrated in the autosampler
Automatic introduction of solid samples as slurries
Full software control User Benefits:
Reduced sample preparation and analysis time
Reduced potential for contamination
Easy operation
What else can PerkinElmer offer?
Sample Preparation Solutions
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Multiwave 3000 High Pressure Asher (HPA)
Flow Injection Technology (FIAS)
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For sample pre-treatment Hydride generation
Stand-alone Mercury systems (FIMS)
Sample Introduction Systems
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Autodilutors Laser Ablation systems
World class service and support
Inorganic sample preparation….
Multiwave 3000
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Reduced digestion times
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Superior digestion quality Time-saving Easy operation Maximum safety
High Pressure Asher
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Complete sample mineralization
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Minimum organic residue No elemental losses No contamination Multiwave 3000 HPA system
…a clear solution for sample preparation !
FIAS – Flow Injection Systems
2 Models
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FIAS 100 (1 valve, 1 pump) FIAS 400 (1 valve, 2 pumps) Automated sampling for Flame AA
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Dilution
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Add reagents or modifiers Matrix removal Preconcentration Improved sample handling
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Small sample volumes
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High solids samples Hydride generation
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Determination of As, Se, Te, Be, Sb, Sn FIAS 100 system FIAS 400 system
Flow Injection Mercury Systems
FIMS 400
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Determines Mercury via Cold Vapor AA (CVAA)
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Small footprint Fully automated Easy to operate Stand alone system Cost effective Now with WinLab32 for AA software
AAnalyst 600
Conclusions
Not just another AA!
No compromises!
Easiest, simplest AA furnace
Full automation
Full range of accessories
Power of AA WinLab32 software
Ultimate in performance
The AA instrument to take you beyond 2000...